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Crosslinked Fluid Systems

Advanced high-temperature and environmentally friendly solutions

i) Hi Temp Crosslinked Fluid

  • Fluid test up to 311°F stable > 2 hours above 200 cP and breaks below 50 cP prior to well flow back.
  • Borate crosslinked fluid with Guar and HPG polymer. Diesel and Mineral Oil were used to make a polymer slurry
  • HPG polymer for faster and complete hydration.
    • Produces lower insoluble residue compared to native guar, contributing to better proppant pack conductivity
  • Utilizing Sulphur based and/or non-Sulphur Hi Temp Gel Stabilizer
  • CMHPG polymer for superior thermal stability and exhibits excellent stability and performance across a wider range of pH conditions
Hi Temp Crosslinked Fluid Systems
Environmentally Crosslinked Fluid

ii) Environmentally Crosslinked Fluid

Lab Test & Implementation
  • Part of requirement of Green Completion by BP Oman
  • A Green Completion is a zero-flaring concept – hydrocarbon during well test operations are "Cleaned" and then routed to processing facilities for export rather than being flared. The testing removes contaminants – proppant, frac fluid and H2S
  • H2S was a byproduct of Sulphur based Hi Temp Gel Stabilizer in the frac fluid
  • Gel slurry was formulated using mineral oil instead of diesel & non-Sulphur Hi Temp Gel Stabilizer
  • Frac fluid requirement at 300 cP for 3 hours stability
  • 13,000 bbls of AF40XLMO successfully pumped to carry ~ 1M lbs of 20/40 HSP proppant in a single job in 2020 as the 1st frac job with international client in Oman done by Local Omani Frac Service provider

HVFR (High Viscosity Friction Reducer)

Lab Test & Implementation
  • HVFR Slick water fluid system was used to hydraulic fracture Athel Silicilyte formation.
  • Small size proppant (100 mesh & 30/50 ISP) designed to pump 105 MT of proppant per stage up to 3 PPA
  • Completed 10 stages MSF CH Plug & Perf in Sept & Oct 2023
  • Recent development of using special HVFR product that compatible with high TDS water/produced water. The product was successfully pumped in the last well in Nov 2024
  • More wells in the future are planned to be stimulated using produced water with this HVFR
HVFR Wellbore Application HVFR HPHT Test Chart
2

AFCIP: Scale Inhibitor Proppant

Infused ceramic proppant technology for scale prevention
AFCIP Scale Inhibitor Proppant AFCIP Performance Data AFCIP Technology
Key Implementation Details:
  • The field prone to self-scaling issue, from water analysis, the dominant scale is CaCO3
  • Scale reduced the production rate of the well, even more lifetime of the well productivity
  • Scale also create trouble on ESP, as such the costly workover for ESP maintenance needed
  • Implementation of SI strategy will prolong the ESP lifetime, and maintain well production above economics threshold
  • Nominated SI technology is infused inside ceramic proppant
  • Client approved and successfully pumped in 5 wells
3

AFCCP: Self Consolidated Proppant

Screenless completion technology for sand control
Why Screenless Completion?

Rock with UCS less than 1000 psi; P-wave sonic transit time >100 µ.sec/ft; obvious solids and sand production

  • Reduced skin – better productivity
  • Rigless completion and recompletion, minimize cost
  • Full wellbore accessibility, better reservoir management and maintenance
  • Cased hole logging
  • Future conformance control
  • Slim hole, smaller wellbore or monobore
  • Ultimate screenless sand control strategy: TSO Fracturing with proppant flowback control club with chemical consolidation
AFCCP Self Consolidated Proppant
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AFDP: Degradable Particulate Diverter

Advanced diversion technology for multistage fracturing
AFDP Degradable Particulate Diverter Technology AFDP Degradable Particulate Diverter
Most Popular Features of Hydraulic Fracturing:
  • Degradable Particulate Diverter (AFDP), engineered shape, blend & degradation period.
  • Through tubing and WHIT conveyance, eliminate pre & post workover Rig/Hoist less intervention. Alternative solution to costly mechanical diversion techniques (i.e. MSS Frac sleeves, Perf & Plugs, CT conveyance frac treatment, Pinpoint fracturing).
  • Improve reservoir contact, especially important for tight rock formation fracturing.
  • Enabler for multistage fracturing placement across different stress contrast.
  • Far field diversion for geometry control, i.e. frac hit avoidance, height growth control.
  • Improve perforation breakdown. Accommodate all possible perforation shapes.
  • On-the-fly delivery, provide flexibility of real time concentration adjustment.
5

Carbonate Proppant Frac

Specialized solutions for tight carbonate formations

Design Comparison

Several candidate wells screening with target zone of Late Cretaceous tight carbonate formation

  • Various well and reservoir scenario were simulated to cover uncertainty and provide fair comparison: Pore pressure depletion, YMES, Stress contrast and anisotropy, permeability and fluid efficiency, tubular friction, perforation interval
  • Initially gelled acid and crosslinked Self-Diversion Acid were chosen for fluid system for contractual context. Retarded emulsified acid system were implemented on later phase of the campaign
  • For comparison, equivalent budgetary job size between acid fracturing and propped fracturing were simulated
  • For average candidates, the study indicate propped fracturing provide better conductive fracture penetration, therefore more flow area. However, some pre-existing completion can only be stimulated proppantless.
Carbonate Proppant Frac Design Carbonate Proppant Frac Design Analysis
Carbonate Proppant Frac Execution Carbonate Proppant Frac Execution Analysis

Execution

Series of prejob injection decline pumping were performed to include:

  • BDT and DFIT with small volume brine
  • SRT with brine in the case of high NWB suspected
  • FET calibration injection with crosslinked fluids if excessive leak-off anticipated
  • Largely, the secondary leakoff due to fissures opening is anticipated at Field L, M & S
  • Some jobs with RA Tracers run confirmed the fracture height as pressure matched post job, however for the well with lack of cement isolation this can be misleading
  • Acid frac treatment was performed at Field S (gel acid) & M (emulsified acid), to complement study comparison.

Post Fracture Evaluation

Master databases were collected to include critical information:

  • Well & reservoir data
  • Design & actual treatment parameter
  • Pressure, rate data and diagnostics
  • Other operational parameter

Following the fracturing campaign:

  • Substantial improvement in both gross and net oil production (oil production increased by a factor of 20).
  • Productivity was sustained, uptime improved from 25% to 100%.
  • Propped fracturing method is preferred when applicable, while retarded acid fracturing provide more flexibility for complex pre-existing well completion
Carbonate Proppant Frac Evaluation Carbonate Proppant Frac Performance
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Emulsified Acid System

Retarded acid reaction for deep penetration
Emulsified Acid System

Emulsified Acid System

  • Oil-in-acid emulsions where acid droplets are encapsulated by a continuous oil phase, stabilized by surfactants.
  • The oil phase retards the acid's reaction with the formation, allowing deeper penetration and more effective etching (wormholing) in carbonate reservoirs.
  • Retarded reaction, reduced fluid loss, inherent diverting capabilities, and enhanced corrosion protection.
  • Primarily for matrix acidizing in deep or fractured carbonate formations requiring extended acid contact.
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Crosslinked Acid System

High-viscosity gelled acid for superior diversion

Crosslinked Acid System

  • Aqueous acid solutions viscosified by polymers and then crosslinked with metal ions to form a high-viscosity gel.
  • Superior Diversion: The high viscosity helps divert acid away from high-permeability streaks and into less permeable, undamaged zones, ensuring more uniform treatment.
  • Reduced Fluid Loss: The viscous nature helps minimize fluid leak-off.
  • Extended Reaction Time: The increased viscosity can also slightly slow down the acid reaction, though less dramatically than emulsified systems
  • Acid fracturing treatments in carbonates where both fracture creation and deep acid etching are desired.
  • Focus on diversion and fracture conductivity through increased viscosity
Crosslinked Acid System

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